Wimbledon champion Carlos Alcaraz tumbled out of the Cincinnati Open after losing in three sets to world No.46 Gael Monfils.
Alcaraz could make little impact when the round of 32 match resumed on Friday.
Rain had forced the players off on Thursday night with Alcaraz a set up but 3-1 down in a second set tie-break.
Frenchman Monfils was quickly out of the blocks to level the contest, and he then took the decider for a 4-6 7-6 (7-5) 6-4 triumph.
Alcaraz’s frustration with his performance surfaced in the deciding set as he smashed his racket after missing an opportunity to break 37-year-old Monfils’ serve.
Alcaraz was making his first hard-court appearance since March, since when he has won the French Open, Wimbledon and a silver medal at the Paris Olympics.
Third seed Alexander Zverev reached the quarter-finals with a 7-5 7-6 (8-6) victory over Spain’s Pablo Carrero Busta.
And Andrey Rublev enjoyed a comfortable passage to the last-eight, defeating American Brandon Nakashima 7-6 (7-5) 6-1.
Rublev will now play world No.1 Jannik Sinner in the quarter-finals, whose third-round opponent, Australia’s Jordan Thompson, withdrew before their match because of a rib injury.
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